WebEntry Amine Work-up Yield (%) Relative Mol. E% 1 pyrrolidine aqueous; then column 91 4a 1 2 pyrrolidine column 75 4a 1.4 3 aniline precipitate 72 5a 24 4 benzylamine precipitate 81 6a 28 With the optimized reaction and isolations procedure in hand, the reaction of aniline (3b) and benzylamine (3c) with acid chlorides 2 was investigated (Scheme 2). http://eprints.hud.ac.uk/id/eprint/30317/3/JECamp%202416%20EJOC.pdf
Synthesis of amides from acid chlorides and amines in the bio …
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